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Question: chm 2260 organic chemistry laboratory analytical data sheet for experiment...

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CHM 2260 Organic Chemistry laboratory Analytical Data Sheet for Experiment 1 (Aspirin synthesis) Structure Yieldle and%) Acetylsalicylic acid (Aspirin) la Ho1o Formula TLC R value Molar Mass TLC eluant Color and Form Melting PointC] d 5 H NMR (300 MHz, solvent CDC MR (300 MHz, solvent CDC) δ [ppm] | Multiplicity | # of H . Peak assign. δ [ppm] . Peak assignment 8.1 7.6 7.3 7.1 5.05 2.3 170 169 151 135 132 126 124 122 21 MS FT-IR (NaCl plate, thin film) m/t | % relative | lon assignment wavenumber lem ] | Bond assignment intensity (structure of ion 3100 1790 1700 1600 1200 180 120
CHM 2260 Organic Chemistry Laboratory I Analytical Data Sheet for Experiment 2 (Microwave Amidation) Structure Yield (g and %) ! Compound Name TLC R Formula CH TLC eluent Molar Mass [&/mol] Melting Point C Color and Form H NMR C NMR Atom assign 6 (ppm) 24.84 116.77 120.11 122.44 130.98 133.75 140.90 168.29 169.33 Multiplicity! |Atom assign #H 61ppm) 2.15 7.15 7.58 7.99 8.5 11.1 GC-MS FT-IR (NaCI plate, thin film) lon assignment Wavenumber (cm)Bond assignment 3100-2500 2909 m/21 %relative intensity structure of ion 179 1646 1604, 1450 1578 137 43
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